Hydrothermal Synthesis of Superfine Strontium Titanate Particles

Qian Qian; Yin Liu; Chen Chen; Peiliang Zhang; Baoxiang Jiao; Guihua Hou

doi:10.14233/ajchem.2014.17311

Issue

Vol. 26 No. 6 (2014): Vol 26 Issue 6

Issue Published : March 10, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Hydrothermal Synthesis of Superfine Strontium Titanate Particles

https://doi.org/10.14233/ajchem.2014.17311

Qian Qian

School of Materials Science and Engineering, Anhui University of Science and Technology, Huainan 232001, Anhui Province, P.R. China

Yin Liu

School of Materials Science and Engineering, Anhui University of Science and Technology, Huainan 232001, Anhui Province, P.R. China

Chen Chen

School of Materials Science and Engineering, Anhui University of Science and Technology, Huainan 232001, Anhui Province, P.R. China

Peiliang Zhang

School of Materials Science and Engineering, Anhui University of Science and Technology, Huainan 232001, Anhui Province, P.R. China

Baoxiang Jiao

School of Materials Science and Engineering, Yancheng Institute of Technology, Yancheng 224051, Jiangsu Province, P.R. China

Guihua Hou

School of Materials Science and Engineering, Yancheng Institute of Technology, Yancheng 224051, Jiangsu Province, P.R. China

Corresponding Author(s) : Yin Liu

yinliu@aust.edu.cn

Asian Journal of Chemistry, Vol. 26 No. 6 (2014): Vol 26 Issue 6
Article Published : March 12, 2014

Abstract

The superfine strontium titanate (SrTiO₃) particles was successfully synthesized by hydrothermal method using KTiO(C₂O₄)₂·3H₂O, Sr(NO₃)₂ as raw materials and NaOH as mineralizer. The as-prepared samples were examined by X-ray powder diffraction for crystalline phase identification and scanning electron microscopy for particles morphology. The results show that the single phase of SrTiO₃ could be obtained at 200 ºC for 12 h as the molar ratio of raw materials and mineralizer was 1:6. The hydrothermal temperature was the main reason which affected the crystal growth rate.

Keywords

Strontium titanate Microstructure Hydrothermal method

Qian, Q., Liu, Y., Chen, C., Zhang, P., Jiao, B., & Hou, G. (2014). Hydrothermal Synthesis of Superfine Strontium Titanate Particles. Asian Journal of Chemistry, 26(6), 1645–1647. https://doi.org/10.14233/ajchem.2014.17311

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References

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References

C.X. Yang, T.Y. Liu, Z.J. Cheng, H.X. Gan and J.Y. Chen, Physica B, 407, 844 (2012); doi:10.1016/j.physb.2011.12.020.

P. Blennow, K.K. Hansen, L.R. Wallenberg and M. Mogensen, J. Eur. Ceram. Soc., 27, 3609 (2007); doi:10.1016/j.jeurceramsoc.2007.02.009.

C.-A. Chang, B. Ray, D.K. Paul, D. Demydov and K.J. Klabunde, J. Mol. Catal. Chem., 281, 99 (2008); doi:10.1016/j.molcata.2007.08.014.

H.W. Kang, S.N. Lim, D. Song and S.B. Park, Int. J. Hydrogen Energy, 37, 11602 (2012); doi:10.1016/j.ijhydene.2012.05.020.

F. Zou, Z. Jiang, X.Q. Qin, Y.X. Zhao, L.Y. Jiang, J.F. Zhi, T.C. Xiao and P.P. Edwards, Chem. Commun., 48, 8514 (2012); doi:10.1039/c2cc33797e.

B.R. Sudireddy, P. Blennow and K.A. Nielsen, Solid State Ion., 216, 44 (2012); doi:10.1016/j.ssi.2011.11.025.

X. Li, H.L. Zhao, F. Gao, N. Chen and N.S. Xu, Electrochem. Commun., 10, 1567 (2008); doi:10.1016/j.elecom.2008.08.017.

X. Li, H.L. Zhao, W. Shen, F. Gao, X.L. Huang, Y. Li and Z.M. Zhu, J. Power Sources, 166, 47 (2007); doi:10.1016/j.jpowsour.2007.01.008.

X. Li, H. Zhao, X. Zhou, N. Xu, Z. Xie and N. Chen, Int. J. Hydrogen Energy, 35, 7913 (2010); doi:10.1016/j.ijhydene.2010.05.043.

H.-L. Li, Z.-N. Du, G.-L. Wang and Y.-C. Zhang, Mater. Lett., 64, 431 (2010); doi:10.1016/j.matlet.2009.11.040.

Y.- Liu, Y.- Lu, M. Xu, L.- Zhou and S.- Shi, Mater. Chem. Phys., 114, 37 (2009); doi:10.1016/j.matchemphys.2008.05.101.

H. Yu, S.X. Ouyang, S.C. Yan, Z.S. Li, T. Yu and Z.G. Zou, J. Mater. Chem., 21, 11347 (2011); doi:10.1039/c1jm11385b.

T. Puangpetch, T. Sreethawong, S. Yoshikawa and S. Chavadej, J. Mol. Catal. Chem., 287, 70 (2008); doi:10.1016/j.molcata.2008.02.027.

Y.H. Chen and Y.D. Chen, J. Hazard. Mater., 185, 168 (2011); doi:10.1016/j.jhazmat.2010.09.014.

A. Huang, A.D. Handoko, G.K.L. Goh, S.R. Shannigrahi and C.K. Tan, Progr. Cryst. Growth Charact. Mater., 57, 109 (2011); doi:10.1016/j.pcrysgrow.2011.10.003.

Issue

Vol. 26 No. 6 (2014): Vol 26 Issue 6

Hydrothermal Synthesis of Superfine Strontium Titanate Particles

Corresponding Author(s) : Yin Liu

Abstract

Keywords

Full Article

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