Synthesis and Structure of bis(2,5-Dioxopyrrolidin-1-yl)adipate

Jingyu Zhang1; Xuan Zhao1; Xuehui Hou2

doi:10.14233/ajchem.2014.18358

Issue

Vol. 26 No. 24 (2014)

Issue Published : 1 December 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Synthesis and Structure of bis(2,5-Dioxopyrrolidin-1-yl)adipate

https://doi.org/10.14233/ajchem.2014.18358

Jingyu Zhang1

1School of Pharmacy Henan University of Traditional Chinese Medicine, Zhengzhou 450008, P.R. China 2Department of Quality Detection and Management, Henan University of Animal Husbandry and Economy, Zhengzhou 450011, P.R. China *Corresponding author: Tel/Fax: +86 371 86176305; E-mail: houxh2006@163.com

Xuan Zhao1

Xuehui Hou2

Corresponding Author(s) : Jingyu Zhang1

Asian Journal of Chemistry, Vol. 26 No. 24 (2014)
Article Published : 2 December 2014

Abstract

bis(2,5-Dioxopyrrolidin-1-yl)adipate was prepared from adipate. Its structure was determined by single crystal X-ray diffraction analysis. The crystals are monoclinic space group P2₁/c with a = 5.2972(3), b = 7.5196(5), c = 19.2660(13) Å, a = 90.00, b = 99.776(6), g = 90.00°, V = 756.28(8) Å³, Z = 2, F(000) = 356.0, D_c = 1.494 g/cm³, μ = 1.070 mm^-1, the final R = 0.0511 and wR = 0.1135. A total of 2484 reflections were collected, of which 1342 were independent (R_int = 0.0255).

Keywords

Adipate derivative Synthesis Crystal structure.

Zhang1, J., Zhao1, X., & Hou2, X. (2014). Synthesis and Structure of bis(2,5-Dioxopyrrolidin-1-yl)adipate. Asian Journal of Chemistry, 26(24), 8569–8571. https://doi.org/10.14233/ajchem.2014.18358

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References

M.R. Jakobsen, J. Haasnoot, J. Wengel, B. Berkhout and J. Kjems, Retrovirology, 4, 29 (2007).

L. Dong, L. Zuo, S. Xia, S. Gao, C. Zhang, J. Chen and J. Zhang, J. Gene Med., 11, 229 (2009).

N. Kipshidze, P. Iversen, E. Keane, D. Stein, P. Chawla, V. Skrinska, L.R. Shankar, R. Mehran, V. Chekanov, G. Dangas, R. Komorowski, C. Haudenschild, A. Khanna, M. Leon, M.H. Keelan and J. Moses, Cardiovasc. Radiat. Med., 3, 26 (2002).

J.F. Schlaak, A.P. Barreiros, S. Pettersson, P. Schirmacher, K.-H. Meyer Zum Buschenfelde and M.F. Neurath, ZumBüschenfelde J. Scand. Immunol., 54, 396 (2001).

D.E. Fonseca and J.N. Kline, Adv. Drug Deliv. Rev., 61, 256 (2009).

J.Y. Zhang, D. Lu, A.X. Li, J. Yang and S.Q. Wang, Tetrahedron Lett., 55, 94 (2014).

(a) G.M. Sheldrick, Acta Crystallogr., 64A, 112 (2008); (b) G.M. Sheldrick, Acta Crystallogr., 64A, 112 (2008); (c) O.V. Dolomanov, L.J. Bourhis, R.J. Gildea, J.A.K. Howard and H. Puschmann, J. Appl. Cryst., 42, 339 (2009).

D. Cremer and J.A. Pople, J. Am. Chem. Soc., 97, 1354 (1975).

Author biographies is not available.