Purification of Two Flavones from Chamaecyparis obtusa by Solid-Phase Extraction

Y.R. Lee; K.H. Row

doi:10.14233/ajchem.2014.15805

Issue

Vol. 26 No. 10 (2014): Vol 26 Issue 10

Issue Published : May 10, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Purification of Two Flavones from Chamaecyparis obtusa by Solid-Phase Extraction

https://doi.org/10.14233/ajchem.2014.15805

Y.R. Lee

Department of Chemical Engineering, Inha University, Incheon, Republic of Korea

K.H. Row

Department of Chemical Engineering, Inha University, Incheon, Republic of Korea

Corresponding Author(s) : K.H. Row

rowkho@inha.ac.kr

Asian Journal of Chemistry, Vol. 26 No. 10 (2014): Vol 26 Issue 10
Article Published : May 10, 2014

Abstract

Solid phase extraction was used to purify two compounds obtained by Chamaecyparis obtusa. Commercial silica and amino silica, MCM-41 and amino MCM-41, respectively, which have a regular structure, were applied as sorbents to increase the purification efficiency. The adsorption isotherm confirmed amino MCM-41 to have higher absorption ability. Moreover, the two target compounds could be separated and purified by solid phase extraction using amino MCM-41 with different washing and elution solvents. Under optimal conditions, 4.93 μg/g of myricetin and 5.91 μg/g of amentoflavone were extracted from Chamaecyparis obtusa.

Keywords

Purification Flavones MCM-41 Solid phase extraction

Lee, Y., & Row, K. (2014). Purification of Two Flavones from Chamaecyparis obtusa by Solid-Phase Extraction. Asian Journal of Chemistry, 26(10), 2823–2826. https://doi.org/10.14233/ajchem.2014.15805

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References

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References

S. Koyama, Y. Yamaguchi, S. Tanaka and J. Motoyoshiya, Gen. Pharmacol., 28, 797 (1997); doi:10.1016/S0306-3623(96)00370-9.

Y.M. Zhang, J. Xu, L. Xiao, G.Z. Zeng, Z.H. Sun and N.H. Tan, Molecules, 18, 1255 (2013); doi:10.3390/molecules18011255.

M. Satoru, Y. Shuichiro and Y. Tsuyoshi, J. For. Res., 3, 27 (2003).

M.J. Park, W.S. Choi, H.Y. Kang, K.S. Gwak, G.S. Lee, E.B. Jeung and I.G. Choi, J. Microbiol., 48, 496 (2010); doi:10.1007/s12275-010-9327-2.

E.-J. Hong, K.-J. Na, I.-G. Choi, K.-C. Choi and E.-B. Jeung, Biol. Pharm. Bull., 27, 863 (2004); doi:10.1248/bpb.27.863.

Y. Ohtani, M. Hazama and K. Sameshima, Mokuzai Gakkaishi, 49, 1022 (1997).

M. Tian, D. Han and K.H. Row, Anal. Lett., 44, 737 (2011); doi:10.1080/00032711003783176.

K.C. Ong and H.E. Khoo, Gen. Pharmacol., 29, 121 (1997); doi:10.1016/S0306-3623(96)00421-1.

H.K. Kim, K.H. Son, H.W. Chang, S.S. Kang and H.P. Kim, Arch. Pharm. Res., 21, 406 (1998); doi:10.1007/BF02974634.

I. Erdogan-Orhan, M.L. Altun, B. Sever-Yilmaz and G. Saltan, J. Med. Food, 14, 434 (2011); doi:10.1089/jmf.2010.0053.

Y. Jin and K.H. Row, Korean J. Chem. Eng., 22, 264 (2005); doi:10.1007/BF02701495.

A.R. Khan, M.R. Riazi and Y.A. Al-Roomi, Sep. Purif. Technol., 18, 237 (2000); doi:10.1016/S1383-5866(00)00052-6.

M. Juza, J. Chromatogr. A, 865, 35 (1999); doi:10.1016/S0021-9673(99)00982-6.

Y. Bayrak, Micropor. Mesopor. Mater., 87, 203 (2006); doi:10.1016/j.micromeso.2005.08.009.

C.W. Huck and G.K. Bonn, J. Chromatogr. A, 885, 51 (2000); doi:10.1016/S0021-9673(00)00333-2.

M. Tian, W. Bi and K.H. Row, J. Chem. Technol. Biotechnol., 87, 165 (2012); doi:10.1002/jctb.2670.

M.R. Mello, D. Phanon, G.Q. Silveira, P.L. Llewellyn and C.M. Ronconi, Micropor. Mesopor. Mater., 143, 174 (2011); doi:10.1016/j.micromeso.2011.02.022.

A.M.B. Furtado, Y. Wang, T.G. Glover and M.D. LeVan, Micropor. Mesopor. Mater., 142, 730 (2011); doi:10.1016/j.micromeso.2011.01.027.

A.W. Marczewski, A. Derylo-Marczewska and M. Jaroniec, J. Colloid Interf. Sci., 109, 310 (1986); doi:10.1016/0021-9797(86)90309-7.

Issue

Vol. 26 No. 10 (2014): Vol 26 Issue 10

Purification of Two Flavones from Chamaecyparis obtusa by Solid-Phase Extraction

Corresponding Author(s) : K.H. Row

Abstract

Keywords

Full Article

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